Sodium Iodide → HCID 86738472, compound

HRID 1759158Notes

Reaction equation

HRID 1759158 reaction equation
[CH3:1][CH:2]([CH3:11])[C:3]([P:5](=[O:10])([O:8]C)[O:6][CH3:7])=[O:4].[I-].[Na+:13]>CC(CC)=O>[CH3:1][CH:2]([CH3:11])[C:3]([P:5](=[O:8])([O-:10])[O:6][CH3:7])=[O:4].[Na+:13]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 12633718HCID 12633718, compound

Product 1

HCID 86738472HCID 86738472, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Dimethyl (2-methyl-1-oxopropyl)phosphonate (10.8 g, 0.06 mol) and sodium iodide (9.0 g, 0.06 mol) were dissolved in ethyl methyl ketone (160 ml) and the solution stirred and refluxed for 16 hours. There was evidence of a precipitate after about 10 minutes refluxing.

Workup

  1. temperaturerefluxed for 16 hours
  2. customafter about 10 minutes
  3. temperaturerefluxing

Sources & evidence

ORD record
ord-7e57abf7b40f487c98b92458c24a9845
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

Loading…