HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Monosodium monoethyl acetylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Diethyl acetylphosphonate | HCID 522997 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | Monosodium monoethyl acetylphosphonate | HCID 23701875 | — |
Reaction Steps
A solution of diethyl acetylphosphonate (5 g, 0.028 mol) and oven-dried sodium iodide (4.2 g, 0.028 mol) in molecular sieve dried ethyl methyl ketone (75 ml) was stirred and refluxed for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339443 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-983cb2f816e6413e874478117333893a |
| Source note | uspto-grants-1982_07 |