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HRID1759159

反应详情

EQUATION

反应方程式

HRID 1759159 的结构方程式

REACTANTS

反应物

2
结构：[I-].[Na+]
HCID5238

Sodium Iodide

INa

结构：CCOP(=O)(OCC)C(C)=O
HCID522997

Diethyl acetylphosphonate

C6H13O4P

PRODUCTS

生成物

1
结构：CCOP(=O)([O-])C(C)=O.[Na+]
HCID23701875

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

A solution of diethyl acetylphosphonate (5 g, 0.028 mol) and oven-dried sodium iodide (4.2 g, 0.028 mol) in molecular sieve dried ethyl methyl ketone (75 ml) was stirred and refluxed for 16 hours.

WORKUP

后处理

  1. temperaturerefluxed for 16 hours