Sodium Iodide → HCID 23701878, compound

HRID 1759161Notes

Reaction equation

HRID 1759161 reaction equation
[C:1]([P:4]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:7])[O:5]C)(=[O:3])[CH3:2].[I-].[Na+:15]>CC(CC)=O>[C:1]([P:4]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:5])[O-:7])(=[O:3])[CH3:2].[Na+:15]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 23264536Methyl acetyl(phenyl)phosphinate

Product 1

HCID 23701878HCID 23701878, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Methyl acetylphenylphosphinate (5.0 g, 0.025 mol) was added to a solution of sodium iodide (3.8 g, 0.025 mol) in molecular sieve dried ethyl methyl ketone (50 ml) and the resulting solution was stirred and refluxed for 15 minutes.

Workup

  1. temperaturerefluxed for 15 minutes

Sources & evidence

ORD record
ord-cb111c3406314b5db8ba23a79db817c8
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

Loading…