Sodium Iodide → HCID 178460688, compound

HRID 1759167Notes

Reaction equation

HRID 1759167 reaction equation
[CH3:1][O:2][C:3]([CH2:5][PH:6](=[O:9])[O:7]C)=[CH2:4].[I-].[Na+:11]>CC(CC)=O>[CH3:1][O:2][C:3]([CH2:5][PH:6](=[O:7])[O-:9])=[CH2:4].[Na+:11]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 178460682HCID 178460682, compound

Product 1

HCID 178460688HCID 178460688, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

A solution of the product of step (a) (0.43 g, 2.87 mmol) and oven dried sodium iodide (0.43 g, 2.87 mol) in distilled ethyl methyl ketone (6 ml) was stirred and refluxed for 16 h.

Workup

  1. temperaturerefluxed for 16 h.

Sources & evidence

ORD record
ord-e6674599506640dc97a6302011cc17a2
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

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