HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzyl ether → HCID 178460687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzyl ether | HCID 7657 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 178473688 | HCID 178473688 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178460687 | HCID 178460687 | — |
Reaction Steps
Procedure as for Example 37 using C6H5CH2ONH2HCl (4.797 g), sodium hydroxide (1.2037 g) and sodium acetylmethylphosphinate (4.331 g), except that the benzyl ether is less soluble in ethanol than hydroxylamine hydrochloride and was dissolved in 300 ml solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339443 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-b8032ad986034d4991c27a27c9777818 |
| Source note | uspto-grants-1982_07 |