Ethanol → HCID 23701872, compound

Participants

Reaction Steps

A mixture of sodium acetylmethylphosphinate (4.3 g) and aniline (3.2 ml) was dissolved in ethanol (200 ml) and allowed to stand for 72 hours over 4 A molecular sieve. The solution was filtered free of the solid phase, evaporated in vacuo and the residue was triturated with ether to give a pale brown solid (6.1 g). The nmr spectrum showed that the crude product contained an aromatic moiety.

Provenance & Evidence