Sodium Iodide → HCID 86738487, compound

HRID 1759172Notes

Reaction equation

HRID 1759172 reaction equation
[CH3:1][O:2][CH:3]([P:6]([CH3:10])(=[O:9])[O:7]C)[O:4][CH3:5].[I-].[Na+:12]>C(C(C)=O)C>[CH3:1][O:2][CH:3]([P:6]([CH3:10])(=[O:7])[O-:9])[O:4][CH3:5].[Na+:12]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 12601977HCID 12601977, compound

Product 1

HCID 86738487HCID 86738487, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

The product of step (a) (7.4 g) in methyl ethyl ketone (75 ml) was refluxed for 2 hr with sodium iodide (7.0 g). The resulting suspension was cooled and the product filtered off, washed and dried (7.4 g). The n.m.r spectrum was consistent with the required material.

Workup

  1. temperatureThe resulting suspension was cooled
  2. filtrationthe product filtered off
  3. washwashed
  4. customdried (7.4 g)

Sources & evidence

ORD record
ord-69a9dc1ff9f342409dc93051741b31a7
Source dataset
uspto-grants-1982_07
Patent number
US04339443

Reaction notes

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