HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butyl-4-butylamino-3,5-dipropyl-1,2,4-triazolium chloride → 1-Butyl-4-butylamino-3,5-dipropyl-1,2,4-triazolium (1,1-dimethyloxyethyl)methylphosphinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butyl-4-butylamino-3,5-dipropyl-1,2,4-triazolium chloride | HCID 20532281 | — |
| Reactant | HCID 86738481 | HCID 86738481 | — |
| Product | 1-Butyl-4-butylamino-3,5-dipropyl-1,2,4-triazolium (1,1-dimethyloxyethyl)methylphosphinate | HCID 86738492 | 76.5% |
Reaction Steps
By the procedure of Example 53 the product of Example 18 (3.8 g) and 1-butyl-4-butylamino-3,5-dipropyl-1,2,4-triazolium chloride (6.0 g) were mixed and the reaction worked up to give the rquired salt as a pale yellow oil (6.5 g). The nmr spectrum was in agreement with the required structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339443 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-f96dec6ecd4e4a19a13591c8b9ef8657 |
| Source note | uspto-grants-1982_07 |