Water → HCID 13067046, compound

Participants

Reaction Steps

To a solution of 1,6-dimethyl-4-(n-dodecylamino)-2-(2-hydroxyethylamino)pyrimidinium iodide (1.19 g, 0.0025 m) in a stirred mixture of water (10 ml) and 2-propanol (10 ml) at room temperature, is added silver acetate (0.44 g, 0.0026 m). An immediate yellow green precipitate forms. After allowing the stoppered mixture to stir overnight, the reaction mixture is filtered and the filtrate is concentrated under reduced pressure at room temperature to yield 1.0 g of 1,6-dimethyl-4-(n-dodecylamino)-2-(2-hydroxyethylamino)pyrimidinium acetate, m.p. 69°-74° C. with some softening at 58° C.

Provenance & Evidence