HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12803422, compound → 1-(2-Methoxyethyl)-4-phenylimidazolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12803422 | HCID 12803422 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(2-Methoxyethyl)-4-phenylimidazolidin-2-one | HCID 12803423 | 91.5% |
Reaction Steps
The 1-(2-methoxyethyl)-4-phenyl-4-imidazolin-2-one (6.5 g) so obtained is next admixed with 10% palladium on carbon (0.7 g) in ethanol (50 ml). The mixture is thereafter hydrogenated at 50 psi at room temperature for four hours and the catalyst is filtered. Resultant filtrate is finally concentrated to yield racemic 1-(2-methoxyethyl)-4-phenyl-2-imidazolidone (6.0 g), [α]D20 =-0.2(c=1 in CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04339603 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-7cec78dbd0884ea285c883ff0da02de3 |
| Source note | uspto-grants-1982_07 |