HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → Styrene butyl acrylate butyl maleate divinylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | 1,2-Diethenylbenzene | HCID 66666 | — |
| Reactant | Mono-n-butyl maleate | HCID 86595084 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Styrene butyl acrylate butyl maleate divinylbenzene | HCID 86738504 | — |
Reaction Steps
50 parts by weight of xylene is placed in a three-necked plask, and 75 parts by weight styrene, 20 parts by weight butyl acrylate, 5 parts by weight butyl maleate, 0.6 parts by weight divinylbenzene and 0.3 parts by weight benzoyl peroxide are added through a dropping funnel under reflux over 3 hours. Then a solution of 0.3 parts by weight benzoyl peroxide in xylene is dropwise added and refluxing is continued for 3 hours followed by cooling and removing the xylene to give a styrene-butyl acrylate-butyl maleate-divinylbenzene copolymer. Gel content of the resulting polymer is 0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04340660 |
| Source dataset | uspto-grants-1982_07 |
| ORD ID | ord-2aeb7482661f4aa6b794e27341f75aff |
| Source note | uspto-grants-1982_07 |