Pyrrolidine → HCID 12152135, compound

Participants

Reaction Steps

4.79 g (0.021 mol) of 6-chloro-2-methoxy-3-nitropyridine, 40 ml of ethanol and 3.5 ml (0.042 mol) of pyrrolidine are charged to a fully equipped round-bottomed flask. The mixture is brought to reflux for 1 hour with stirring and then the mixture is cooled to ambient temperature. The product which crystallizes is filtered off and then washed with diisopropyl ether. After drying, 4.6 g of yellow powder are obtained, Yd: 96%.

Provenance & Evidence