HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxypyrrolidine → HCID 12152136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxypyrrolidine | HCID 98210 | — |
| Reactant | 6-Chloro-2-methoxy-3-nitropyridine | HCID 10797703 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12152136 | HCID 12152136 | 78.9% |
Reaction Steps
2 g (0.0106 mol) of 6-chloro-2-methoxy-3-nitropyridine, 25 ml of ethanol and 1.9 g of 3-pyrrolidinol are charged to a fully equipped round-bottomed flask. The mixture is brought to 50° C. for one hour with stirring and the mixture is poured onto an ice/water mixture with stirring. The precipitate formed is filtered off and dried. 2 g of yellow powder are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06837908B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-2ae9a172663d42a0b6e6f1b751aa9cc9 |
| Source note | uspto-grants-2005_01 |