Ethanol → HCID 22598782, compound

Participants

Reaction Steps

4 g (0.02 mol) of 6-chloro-2-methoxy-3-nitropyridine, 60 ml of ethanol and 4.2 ml of piperidine are charged to a fully equipped round-bottomed flask. The mixture is brought to reflux for two hours with stirring and then the mixture is poured onto an ice/water mixture with stirring. The precipitate formed is filtered off and dried. 2 g of yellow powder are obtained, Yd=42.5%.

Provenance & Evidence