HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzaldehyde → 265113-47-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | 4-(Methylsulfonyl)aniline | HCID 79617 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 265113-47-1 | HCID 11097838 | — |
Reaction Steps
A mixture of 19.60 g (115 mmol) of 4-methylsulfonylaniline, 12.19 mL (115 mmol) of 4-fluorobenzaldehyde and 590 mL of toluene was refluxed in a Dean-Stark for 2 days. The solvent was removed and the crude product obtained was directly used in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06838476B1 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-a20ef69699cf4e3296d198b4a78421e2 |
| Source note | uspto-grants-2005_01 |