Hydrochloric Acid → HCID 178508634, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 350 mg of 9-(6-methoxy-3-pyridyl)-8-(2-pyridyl)-9H-6-purineamine and 6 mL conc. aqueous hydrochloric acid was stirred at 105° C. for 1 hour and 45 minutes. From the resulting yellowish brown oily material, the solvent was evaporated, whereby yellowish brown crystals were obtained. The resulting crystals were collected by filtration with ethanol, to give 77 mg of the title compound as brown crystals (23% y.).

Provenance & Evidence