HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Carboxyethoxy)benzoic acid → HCID 13316012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Carboxyethoxy)benzoic acid | HCID 13316009 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 13316012 | HCID 13316012 | 70% |
Reaction Steps
3-(4-Carboxyphenoxy)propionic acid (2.5 g) [prepared according to the procedure of J. Lichtenberger and R. Geyer. Bull. Soc. Chim. Fr., 1963 275] in conc. sulfuric acid (20 ml) was heated to 100° C. for 4 h and then poured onto crushed ice. The resultant precipitate was filtered and dried in vacuo to give the title compound (1.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06841560B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-e509a9274bbe4f3483969bfa6195ecfa |
| Source note | uspto-grants-2005_01 |