HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Thioglycolate → HCID 54725334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Thioglycolate | HCID 12185 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 136116400 | HCID 136116400 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 54725334 | HCID 54725334 | — |
Reaction Steps
Treatment of 5-ethyloxycarbonyl-2-methylthio-4-phenyl-6-oxopyrimidine (63 mg) with POCl3 (304 μl) and subsequent reaction of the product with ethyl 2-mercaptoacetate were performed according to the methods described in example 1. The pure title compound was obtained after chromatography on silicagel in heptane/ethyl acetate 100/0=>60/40 (v/v) as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06841553B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-e04f01ddcb9548cdaf5f60a3c46246f3 |
| Source note | uspto-grants-2005_01 |