Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1760708Generated: October 28, 2026

HCID 21912199, compound → HCID 21912168, compound

https://huagongshe.com/reaction/1760708

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21912199HCID 21912199—
ReactantHCID 178418287HCID 178418287—
SolventDichloromethaneHCID 6344—
ProductHCID 21912168HCID 21912168—

Reaction Steps

The title compound was prepared by oxidation of 4-chloro-6-methyl-2-(2,4,6-trimethyl-phenoxy)-pyridin-3-yl-methanol with pyridinium chlorochromate in methylene chloride at room temperature. The desired product was isolated after column chromatography to give a green solid (80% yield). 1H NMR(CDCl3) d 10.66(s, 1H), 6.91(s,3H), 2.31(s,3H), 2.07(s,3H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06844351B1
Source datasetuspto-grants-2005_01
ORD IDord-5eba9c4fcecc46fca6ec37bbed998bea
Source noteuspto-grants-2005_01