HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 69532064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | 4-(Dodecyloxy)-3-methoxybenzaldehyde | HCID 287532 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69532064 | HCID 69532064 | — |
Reaction Steps
4-Dodecyloxy-3-methoxybenzaldehyde (166 g; 0.519 mol) is heated for 2 hours at 100° C. with ammonium acetate (20 g; 0.388 mol) and nitromethane (49 ml; 0.914 mol). The resulting melt is then added dropwise with vigorous stirring to methanol, yellow crystals precipitating. After filtration, the residue is washed several times with methanol and then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06846492B2 |
| Source dataset | uspto-grants-2005_01 |
| ORD ID | ord-81516bae352b4699a83761da706d07a4 |
| Source note | uspto-grants-2005_01 |