HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 20044191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | HCID 13985405 | HCID 13985405 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20044191 | HCID 20044191 | — |
Reaction Steps
The resultant compound of Example 75 (400 mg) dissolved in methanol containing added CHCl3 was hydrogenated over 10% Pd/C (40mg) with 3 atmospheres hydrogen. Filtration and evaporation gave the desired compound (305mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826815 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-a4f8f501a0254fea8f20ad53cae932f5 |
| Source note | uspto-grants-1989_05 |