HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 13770164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Reactant | HCID 70359114 | HCID 70359114 | — |
| Product | HCID 13770164 | HCID 13770164 | — |
Reaction Steps
By reaction of 656 mg of 2-bromo-9,10-didehydro-6-methylergoline-8α-amine (1.5 mmol) with 1,1'-thiocarbonyldiimidazole and diethylamine, as described in Example 11, 535 mg of 3-(2-bromo-9,10-didehydro-6-methyl-8α-ergolinyl)-1,1-diethylthiourea is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826852 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-2f0e1a80994848f39d5da5016879499f |
| Source note | uspto-grants-1989_05 |