HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 178419604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 178502029 | HCID 178502029 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178419604 | HCID 178419604 | 99.9% |
Reaction Steps
A solution of 6.3 parts of methyl [5-[(4-fluorophenyl)hydroxymethyl]-1H-benzimidazol-2-yl]carbamate in 60 parts of acetic acid, saturated with hydrogen bromide was stirred for 3 hours at room temperature. The reaction mixture was evaporated, yielding 9.18 parts (99.9%) of methyl [5-[bromo(4-fluorophenyl)methyl]-1H-benzimidazol-2-yl]carbamate monohydrobromide as a residue (int. 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04826862 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-0028ef86884c4caf9e3f7d5cd0da10dc |
| Source note | uspto-grants-1989_05 |