Phenylhydrazine → HCID 178515174, compound

HRID 1761523Notes

Reaction equation

HRID 1761523 reaction equation
Cl[C:2]1[C:7]([C:8]([O:10]CC)=O)=[CH:6][N:5]=[C:4]2[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][C:3]=12.[C:19]1([NH:25][NH2:26])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:19]1([N:25]2[C:8](=[O:10])[C:7]3[C:2]([C:3]4[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][C:4]=4[NH:5][CH:6]=3)=[N:26]2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 14500574HCID 14500574, compound

Product 1

HCID 178515174HCID 178515174, compound

Procedure

Reaction of ethyl 5,6,7,8,9,10-hexahydro-4-chlorocycloocta[b]pyridine-3-carboxylate with phenylhydrazine according to the procedure analogous to that described in example 1 yields 2,3,6,7,8,9,10,11-octahydro-2-phenylcylcoocta[b]pyrazolo[3,4-d]pyridin-3(5H)-one, m.p. 310°-312°.

Sources & evidence

ORD record
ord-2b5b55f565aa429aa1b1cdf808118e9f
Source dataset
uspto-grants-1989_05
Patent number
US04826854

Reaction notes

Loading…