反应详情

A mixture of 36.5g of 1-[(1,1-dimethyl-2-propenyl)oxy]hexadecane, 23.92 g of m-chloroperbenzoic acid and 225 ml of methylene chloride was stirred overnight. A 7 g portion of m-chloroperbenzoic acid was added, then the mixture was stored in a chill room for 56 hours. This mixture was filtered. The filtrate was washed with dilute aqueous sodium bisulfite, then saturated aqueous sodium bicarbonate, dried and the solvent removed, giving 36 g of the desired compound.

1. waitthe mixture was stored in a chill room for 56 hours
2. filtrationThis mixture was filtered
3. washThe filtrate was washed with dilute aqueous sodium bisulfite
4. dry with materialsaturated aqueous sodium bicarbonate, dried
5. customthe solvent removed