Saccharin → HCID 14255069, compound

Participants

Reaction Steps

4.5 g (0.014 mol) of 1-(2,6-dimethylmorpholin-4-yl)-2-methyl-3-(decahydronaphth-2-yl)-propane and 2.58 g (0.014 mol) of saccharine are dissolved together in 80 ml of acetone and the solution is stirred at room temperature for 15 minutes. After the solvent has been evaporated off, 7 g (100% of theory) of 1-(2,6-dimethylmorpholin-4-yl)-2-methyl-3-(decahydronaphth-2-yl)-propane saccharine salt are obtained as an amorphous solid.

Provenance & Evidence