HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19888656, compound → HCID 19888657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19888656 | HCID 19888656 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19888657 | HCID 19888657 | — |
Reaction Steps
A solution of 2-[N-methyl-N-(5-nitrobenzofur-2-ylmethyl)amino]-5-nitroindane (0.33 g) in ethanol (25 ml) containing 5% Pd/C (0.03 g) was stirred under a hydrogen atmosphere [206.8 kPa (30 p.s.i.)] for 3 hours at room temperature. The catalyst was then removed by filtration and the filtrate evaporated in vacuo to afford the title compound as a gum, yield 0.3 g, which was used directly without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04829071 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-127c9f1e4cb345f287e0b4022f7dfd86 |
| Source note | uspto-grants-1989_05 |