HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14500295, compound → [2-tert-Butyl-4-(4-fluorophenyl)-5-phenylfuran-3-yl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14500295 | HCID 14500295 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | [2-tert-Butyl-4-(4-fluorophenyl)-5-phenylfuran-3-yl]methanol | HCID 14500301 | — |
Reaction Steps
Under a dry nitrogen atmosphere, to a slurry of 1.15 g (30.4 mmol) of lithium aluminum hydride in 50 ml of dry ether at about 0° was added 5.56 g (15.2 mmol) of 4-(4-fluorophenyl)-2-tert.-butyl-5-phenyl-3-furyl-carboxylic acid, ethyl ester in 25 ml of dry ether. The mixture was heated at reflux for one-half hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04829081 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-4a20bd316a8c4a848c1d797cda85f1ae |
| Source note | uspto-grants-1989_05 |