HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylene Glycol → HCID 86743027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylene Glycol | HCID 8117 | — |
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Product | HCID 86743027 | HCID 86743027 | 83.3% |
Reaction Steps
Diethylene glycol (31.8 g, 0.3 mole) and p-nitrobenzoyl chloride (116 g, 0.62 mole) were reacted under the conditions described in Example 1, Part A. The product was crystallized from ethyl acetate to give bis-(4-nitrobenzoyl)-diethylene glycol (101 g) as a pale yellow solid, m.p. 100°-102° C. The product was homogeneous by TLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04829099 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-94871ac009784dadb5313817ca971116 |
| Source note | uspto-grants-1989_05 |