HCID 20042526, compound → HCID 20042530, compound

Participants

Reaction Steps

A mixture of 2-amino-3-(3-methoxymethoxybenzyloxy)pyridine (7.6 g) and 10% sulfuric acid (150 ml) was stirred at room temperature for 4 hours and the resulting precipitates were collected by filtration. The obtained sulfate was treated with an aqueous solution of sodium bicarbonate and the precipitates were collected by filtration, washed with water, and air-dried to give 2-amino-3-(3-hydroxybenzyloxy)pyridine (4.88 g).

Provenance & Evidence