HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic-formic anhydride → 2-Formamido-6-methylbenzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic-formic anhydride | HCID 75269 | — |
| Reactant | (2-Amino-6-methylphenyl)methanol | HCID 15339417 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 2-Formamido-6-methylbenzyl alcohol | HCID 14368452 | 84.9% |
Reaction Steps
Acetic formic anhydride (1.85 g) was added to a solution of 2-amino-6-methylbenzyl alcohol (2.74 g) in benzene (55 ml) at room temperature. After being stirred for 2 hours, the mixture was diluted with n-hexane (10 ml) and the precipitates were collected by filtration to give 2-formamido-6-methylbenzyl alcohol (2.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831041 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-31200514c4f54d2a9954e0aaa3bb2148 |
| Source note | uspto-grants-1989_05 |