HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → 6-Methyl-2-(3-methyl ureido)benzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | (2-Amino-6-methylphenyl)methanol | HCID 15339417 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 6-Methyl-2-(3-methyl ureido)benzyl alcohol | HCID 14368453 | 64.1% |
Reaction Steps
A mixture of 2-amino-6-methylbenzyl alcohol (0.274 g) and methyl isocyanate (0.11 g) in benzene (5.2 ml) was stirred at room temperature for 15 minutes. The resulting precipitates were collected by filtration and dried to give 6-methyl-2-(3-methyl ureido)benzyl alcohol (0.24 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831041 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-3167749fd55e4931b3c06f29c9259668 |
| Source note | uspto-grants-1989_05 |