HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylhexanol → 2-(2-Ethylhexyloxy)-3-tert-butyl-1,3,2-oxazaphospholidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylhexanol | HCID 7720 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-tert-Butyl-2-chloro-1,3,2-oxazaphospholidine | HCID 14228109 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(2-Ethylhexyloxy)-3-tert-butyl-1,3,2-oxazaphospholidine | HCID 20043205 | 81% |
Reaction Steps
The procedure of Example 3 is repeated using 18.16 g (0.10 mol) of 3-tert-butyl-2-chloro-1,3,2-oxazaphospholidine in 115 ml of THF and 13.16 ml (0.10 mol) of triethylamine and 13.2 g (0.10 mol) of 2-ethylhexanol in 115 ml of THF to give 22.3 g (81.0%) of a clear liquid: b.p. 89°-92° C. (0.05 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831178 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-b84f5d07b5db43709e08cbce61a2d974 |
| Source note | uspto-grants-1989_05 |