化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Sulfite → Sodium 3-trifluoromethylbenzylsulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Sulfite | HCID 24437 | — |
| 反応物 | 3-(Trifluoromethyl)benzyl chloride | HCID 69716 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium 3-trifluoromethylbenzylsulfonate | HCID 23700704 | 90.5% |
反応手順
A mixture containing 50 g of 3-trifluoromethylbenzyl chloride and 32.4 g of sodium sulfite in 200 ml of water was refluxed for five hours and then concentrated by evaporation. The concentrate was then filtered to collect the precipitate (product). The precipitate was then washed with ethyl ethyl and then dried in a vacuum oven affording 61 g of sodium 3-trifluoromethylbenzylsulfonate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04831179 |
| 出典データセット | uspto-grants-1989_05 |
| ORD ID | ord-53dd339ef91b40328984b10a9fd39137 |
| 出典メモ | uspto-grants-1989_05 |