HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13934695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(Acetyloxy)-2,4,5-trifluorobenzoic acid | HCID 13934694 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13934695 | HCID 13934695 | — |
Reaction Steps
In 200 ml of benzene was dissolved 6.10 g (0.026 mole) of 3-acetoxy-2,4,5-trifluorobenzoic acid (V), and to the solution was added 15 ml of thionyl chloride and stirred for 4 hours under reflux. After completion of the reaction, benzene and excess thionyl chloride were completely distilled off under reduced pressure to give 3-acetoxy-2,4,5-trifluorobenzoyl chloride (VI).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04831190 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-0593fdcae426490c87afc177a59264dc |
| Source note | uspto-grants-1989_05 |