HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 70393879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | alpha-Cyclohexylcyclohexanemethanamine | HCID 10774245 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70393879 | HCID 70393879 | — |
Reaction Steps
111 Parts of α-cyclohexylcyclohexanemethanamine and 60 parts of sodium carbonate were dispersed in 320 parts of methanol. 54 Parts of methyl bromoacetate were added dropwise to this dispersion. The mixture was stirred at room temperature for 72 hours. The precicitate was separated and the solution was concentrated to dryness, yielding methyl N-[(dicyclohexyl)methyl]glycine quantitatively (int. 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04832732 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-98ba4f0a8a5a466c91f16bb464aa114c |
| Source note | uspto-grants-1989_05 |