Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1762398Generated: November 2, 2026

Sodium Carbonate → HCID 70393879, compound

https://huagongshe.com/reaction/1762398

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
ReactantMethyl bromoacetateHCID 60984—
Reactantalpha-CyclohexylcyclohexanemethanamineHCID 10774245—
SolventMethanolHCID 887—
ProductHCID 70393879HCID 70393879—

Reaction Steps

111 Parts of α-cyclohexylcyclohexanemethanamine and 60 parts of sodium carbonate were dispersed in 320 parts of methanol. 54 Parts of methyl bromoacetate were added dropwise to this dispersion. The mixture was stirred at room temperature for 72 hours. The precicitate was separated and the solution was concentrated to dryness, yielding methyl N-[(dicyclohexyl)methyl]glycine quantitatively (int. 1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04832732
Source datasetuspto-grants-1989_05
ORD IDord-98ba4f0a8a5a466c91f16bb464aa114c
Source noteuspto-grants-1989_05