Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 70393879 | HCID 70393879 | — |
| Product | HCID 86743052 | HCID 86743052 | — |
Reaction Steps
143 Parts of methyl N-[(dicyclohexyl)methyl]glycine were added dropwise to 290 parts of formic acid while cooling to 5° C. Subsequently 90 parts of acetic anhydride were added, and the mixture was kept at room temperature for 48 hours. Destillation under vacuo afforded 154 parts of methyl N-[(dicyclohexyl)methyl]-N-formylglycine (int. 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04832732 |
|---|
| Source dataset | uspto-grants-1989_05 |
|---|
| ORD ID | ord-06e0373d2c984ee49ad216fc4d968d72 |
|---|
| Source note | uspto-grants-1989_05 |
|---|
