m-Chloroperbenzoic acid → HCID 20041105, compound

HRID 1762431Notes

Reaction equation

HRID 1762431 reaction equation
ClC1C=CC=C(C(OO)=[O:9])C=1.[C:12]1([N:18]2[C:27](=[O:28])[C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[N:20]=[C:19]2[S:29][CH2:30][C:31]2[CH:36]=[CH:35][N:34]=[CH:33][CH:32]=2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>C(Cl)(Cl)Cl>[C:12]1([N:18]2[C:27](=[O:28])[C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[N:20]=[C:19]2[S:29]([CH2:30][C:31]2[CH:32]=[CH:33][N:34]=[CH:35][CH:36]=2)=[O:9])[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 14575156HCID 14575156, compound

Product 1

HCID 20041105HCID 20041105, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

0.7 g Of m-chloroperbenzoic acid was added under an ice-cold water cooling to 1.12 g of a solution of 3-phenyl-2(4-pyridylmethylthio)-4(3H)-quinazolinone in 50 ml of chloroform and the stirring was continued for 2 hours.

Sources & evidence

ORD record
ord-34b96759070e48569b3db8c0c73f9939
Source dataset
uspto-grants-1989_05
Patent number
US04833144

Reaction notes

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