HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20040862, compound → HCID 54360501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20040862 | HCID 20040862 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54360501 | HCID 54360501 | — |
Reaction Steps
A mixture of the N-n-butyl-N-methyl-4-(4- benzyloxycarbonylpiperazin-1-yl)butyramide thus obtained (0.187 g.), a 10% palladium-on-charcoal catalyst (0.1 g.) and ethanol (5 ml.) was stirred at laboratory temperature under an atmosphere of hydrogen for 22 hours and then filtered and the filtrate was evaporated to dryness. There was thus obtained as an oil N-n-butyl-N-methyl-4-(piperazin-1-yl)butyramide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833135 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-d71e8072a66c43a09d3daab6663f7e3b |
| Source note | uspto-grants-1989_05 |