HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromide ion → HCID 13747681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromide ion | HCID 259 | — |
| Reactant | 3-Methylxanthine | HCID 70639 | — |
| Reactant | 1-Chloro-5-hydroxy-5-methylhexane | HCID 13747679 | — |
| Reactant | 3-Methyl-1,7-bis(5-oxohexyl)-3,7-dihydro-1H-purine-2,6-dione | HCID 15390931 | — |
| Reactant | HCID 178418332 | HCID 178418332 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13747681 | HCID 13747681 | — |
Reaction Steps
The same compound was also obtained, inter alia, by a one-stage dialkylation of 3-methylxanthine with twice the molar amount of 1-chloro-5-hydroxy-5-methylhexane or by reaction of 1,7-bis-(5-oxohexyl)-3-methylxanthine with two equivalents of methylmagnesium chloride or bromide in anhydrous tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833146 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-80123447f4b14216b63d8c9fec5cc336 |
| Source note | uspto-grants-1989_05 |