Nickel Dichloride → HCID 86743062, compound

Participants

Reaction Steps

152.2 g (1.0 mole) of DBU and 64.8 g(0.5 moles) of anhydrous NiCl2 were subjected to reaction at 180° C. for 4 hours in the absence of a solvent, and the reaction mixture was poured into acetone. The deposited crystals were ricovered therefrom by filtration, washed with acetone and dried, whereby 120.5 g of DBU/NiCl2 complex compound was obtained (yield: 55.5%).

Provenance & Evidence