HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diboron → HCID 14500517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diboron | HCID 6328200 | — |
| Reactant | HCID 14500507 | HCID 14500507 | — |
| Product | HCID 14500517 | HCID 14500517 | 81% |
Reaction Steps
was prepared in 81% yield from 30.6 g (0.11 mol) of 6-bromo-N-(2-hydroxyphenyl)hexanamide according to the procedure of Example 1, part b, except that the amide was added to the diborane (inverse addition). The product was crystallized from acetonitrile by the addition of chloroform and then ether, mp 124°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835180 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-e1d6da5a845449b9ae79185e509166b9 |
| Source note | uspto-grants-1989_05 |