HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromohexanoyl chloride → HCID 14500511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromohexanoyl chloride | HCID 89848 | — |
| Reactant | 4-Amino-3-fluorophenol | HCID 2735919 | — |
| Product | HCID 14500511 | HCID 14500511 | 98% |
Reaction Steps
The 10.9 g (0.09 mol) of 4-amino-3-fluorophenol from above was reacted with 8.96 g (0.04 mol) of 6-bromo-hexanoyl chloride according to the procedure of Example 3, part a. 6-Bromo-N-(2-fluoro-4-hydroxyphenyl) hexanamide was obtained in 98% yield after crystallization from acetonitrile, mp 66°-69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835180 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-416ec1289f8944f4a691df5a1d327e5a |
| Source note | uspto-grants-1989_05 |