Methanol → HCID 86743080, compound

HRID 1762923Notes

Reaction equation

HRID 1762923 reaction equation
[CH2:1]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([OH:22])(=[O:21])=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].CO.C1(C)C=CC(S(O)(=O)=O)=CC=1.[C:36]([NH2:41])(=[O:40])[CH:37]1[O:39][CH2:38]1>C(O)(C)C>[CH2:1]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[S:19]([OH:22])(=[O:20])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[C:36]([NH2:41])(=[O:40])[CH:37]1[O:39][CH2:38]1

Participants

5

Reactant 3

HCID 887MethanolHCID 25457Dodecylbenzenesulphonic acidHCID 86743079HCID 86743079, compound

Product 1

HCID 86743080HCID 86743080, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

233.0 parts by weight of a 70% dodecylbenzenesulfonic acid solution supplied in isopropanol by American Cyanamid is mixed with 415.0 parts by weight of methanol. This solution is then added to 167.5 parts by weight of a 26% glycidamide solution of Example 1 till homogeneous and clear.

Sources & evidence

ORD record
ord-be2bd1836b394f26ba5af1cf99eb2bd0
Source dataset
uspto-grants-1989_05
Patent number
US04835227

Reaction notes

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