HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl 7-(benzyloxy)-1H-indole-2-carboxylate → HCID 13242193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl 7-(benzyloxy)-1H-indole-2-carboxylate | HCID 54453124 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13242193 | HCID 13242193 | 87.9% |
Reaction Steps
Under the conditions of Example 14(C), a solution of 5.4 g of 7-benzyloxyindole-2-carboxylic acid phenyl ester in a mixture of 50 ml of methanol and 30 ml of tetrahydrofuran is hydrogenated and worked up, yielding 3.5 g of 7-hydroxyindole-2-carboxylic acid phenyl ester, mp 156°-157° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835175 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-cc7b107ccf1c4c428834035f3d4e4947 |
| Source note | uspto-grants-1989_05 |