HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70381752, compound → HCID 70381301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70381752 | HCID 70381752 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 70381301 | HCID 70381301 | 89.6% |
Reaction Steps
Under the conditions of Example 14(E), 1.5 g of 4-tert-butylaminoacetyl-7-hydroxyindole-2-carboxylic acid phenyl ester hydrochloride is hydrogenated in a mixture of 40 ml of methanol and 40 ml of tetrahydrofuran and worked up, thus producing 1.35 g of 4-(2-tert-butylamino-1-hydroxy-ethyl)-7-hydroxyindole-2-carboxylic acid phenyl ester hydrochloride, decomposition point 165°-166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835175 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-267fc70491a148059ef435b4126e56ce |
| Source note | uspto-grants-1989_05 |