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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1762964Generated: October 30, 2026

HCID 54416050, compound → HCID 70382016, compound

https://huagongshe.com/reaction/1762964

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54416050HCID 54416050—
SolventDiethyl ether methanolHCID 21864698—
ProductHCID 70382016HCID 70382016153.7%

Reaction Steps

408 mg of 7-benzyloxy-4-(N-benzyl-N-tert-butylaminoacetyl)indole-2-carboxylic acid 2-(morpholino)ethyl ester is hydrogenated under the conditions of Example 14(E) and worked up, thus obtaining 250 mg of 7-hydroxy-4-(1-hydroxy-2-tert-butylaminoethyl)indole-2-carboxylic acid 2-(morpholino)ethyl ester monoacetate, decomposition point 177°-177.5° C. (from methanol/diethyl ether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04835175
Source datasetuspto-grants-1989_05
ORD IDord-6daeccb88e074d288075f7aeb1aefbac
Source noteuspto-grants-1989_05