HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-[2-(1-Benzofuran-3-yl)ethyl]formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | 2-Benzo[b]furan-3-ylethylamine | HCID 12420812 | — |
| Product | N-[2-(1-Benzofuran-3-yl)ethyl]formamide | HCID 13923851 | — |
Reaction Steps
A solution of 121 g of 2-(3-benzo[b]furanyl)-ethylamine and 300 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (Na2SO4), charcoaled and concentrated to give 118 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835276 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-9f4fdd9381e043b59fde473ab24256e6 |
| Source note | uspto-grants-1989_05 |