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HRID1762976

反应详情

EQUATION

反应方程式

HRID 1762976 的结构方程式

REACTANTS

反应物

2
结构：CSCCC#N
HCID548386

3-(Methylsulfanyl)propanenitrile

C4H7NS

结构：N=C(N)Nc1nc(CSCCC(=N)NS(N)(=O)=O)cs1
HCID178418935

未命名化合物

PRODUCTS

生成物

1
结构：C=CC(=N)NS(N)(=O)=O
HCID178458073

未命名化合物

PROCEDURE

实验过程

N-sulfamyl-acrylamidine was prepared by a four-step procedure from 3-(methylthio)-propionitrile, with an extremely low (5.5%) yield in several days. The products of the subsequent steps, including famotidine, were isolated by column chromatography.

WORKUP

后处理

  1. customyield in several days
  2. customwere isolated by column chromatography